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HRID20667

反应详情

EQUATION

反应方程式

HRID 20667 的结构方程式

REACTANTS

反应物

2
结构：COC(=O)CBr
HCID60984

Methyl bromoacetate

C3H5BrO2

结构：COc1ccc2c(Nc3c(Cl)cncc3Cl)cc(=O)oc2c1O
HCID24849570

未命名化合物

PRODUCTS

生成物

1
结构：COC(=O)COc1c(OC)ccc2c(Nc3c(Cl)cncc3Cl)cc(=O)oc12
HCID24849710

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from methyl 2-bromoacetate and 4-(3,5-dichloropyridin-4-ylamino)-8-hydroxy-7-methoxy-2H-chromen-2-one (Example 29) following the procedure outlined in Example 25. 1H NMR (400 MHz, DMSO-d6): δ 9.54 (s, 1H), 8.83 (s, 2H), 7.97 (d, 1H), 7.23 (d, 1H), 4.73 (s, 2H), 4.66 (s, 1H), 3.92 (s, 3H), 3.69 (s, 3H); MS (ESI): 424.8.