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HRID20682

反应详情

EQUATION

反应方程式

HRID 20682 的结构方程式

REACTANTS

反应物

2
结构：CC(=O)[O-].[K+]
HCID517044

Potassium acetate

C2H3KO2

结构：COc1ccc2c(Nc3c(Cl)cncc3Cl)cc(=O)oc2c1OCCCCCBr
HCID24849569

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccc2c(Nc3c(Cl)cncc3Cl)cc(=O)oc2c1OCCCCCOC(C)=O
HCID24849842

未命名化合物

PROCEDURE

实验过程

The title compound can be prepared from potassium acetate and 8-(5-bromopentyloxy)-4-(3,5-dichloropyridin-4-ylamino)-7-methoxy-2H-chromen-2-one (Example 28) following the procedure outlined in Example 52. 1H NMR (400 MHz, DMSO-d6): δ 9.53 (s, 1H), 8.83 (s, 2H), 7.95 (d, 1H), 7.22 (s, 1H), 4.65 (s, 1H), 4.00 (m, 4H), 3.93 (s, 3H), 2.00 (s, 3H), 1.73-1.52 (m, 6H); MS (ESI): 480.9.