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HRID2070407

反应详情

EQUATION

反应方程式

HRID 2070407 的结构方程式

REACTANTS

反应物

4
结构：[H-].[Na+]
HCID24758

Sodium hydride

HNa

结构：C1COCCOCCOCCOCCO1
HCID36336

1,4,7,10,13-Pentaoxacyclopentadecane

C10H20O5

结构：Cc1nn(C)c(Cl)c1S(=O)(=O)Cl
HCID2777126

5-chloro-1,3-dimethyl-1H-pyrazole-4-sulfonyl chloride

C5H6Cl2N2O2S

结构：Cc1c(C=O)c[nH]c1-c1ccccc1
HCID71362812

4-Methyl-5-phenyl-1H-pyrrole-3-carbaldehyde

C12H11NO

PRODUCTS

生成物

1
结构：Cc1nn(C)c(Cl)c1S(=O)(=O)n1cc(C=O)c(C)c1-c1ccccc1
HCID86620766

未命名化合物

PROCEDURE

实验过程

By a reaction under similar conditions as in Reference Example 65 and using 4-methyl-5-phenyl-1H-pyrrole-3-carbaldehyde (185 mg), sodium hydride (60% in oil, 60 mg), 15-crown-5 (0.30 mL) and (5-chloro-1,3-dimethyl-1H-pyrazol-4-yl)sulfonyl chloride (298 mg), the title compound was obtained as an oil (yield 379 mg, about 100%).

WORKUP

后处理

  1. customBy a reaction under similar conditions as in Reference Example 65