HRID2070987

反应详情

EQUATION

反应方程式

HRID 2070987 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

3

PROCEDURE

实验过程

To 3-tert-butylbenzonitrile (400 mg) in MeOH (5 mL), aqueous ammonium hydroxide (1 mL) and Raney Nickel (catalytic) were added and the reaction mixture was hydrogenated at 50 psi for 2 h. Then the reaction mixture was filtered and solvent evaporated. (3-tert-butylphenyl)methanamine was used without any purification.

WORKUP

后处理

  1. filtrationThen the reaction mixture was filtered
  2. customsolvent evaporated
  3. custom(3-tert-butylphenyl)methanamine was used without any purification