Ammonium Acetate → HCID 53712444, compound

HRID 2073747Notes

Reaction equation

HRID 2073747 reaction equation
[CH2:1]([N:3]([CH2:19][CH3:20])[CH2:4][C:5]([C:7]1[CH:12]=[C:11]([O:13][CH3:14])[C:10]([O:15][CH3:16])=[C:9]([O:17][CH3:18])[CH:8]=1)=O)[CH3:2].C([O-])(=O)C.[NH4+].[BH3-]C#[N:28].[Na+]>>[CH2:1]([N:3]([CH2:19][CH3:20])[CH2:4][CH:5]([C:7]1[CH:12]=[C:11]([O:13][CH3:14])[C:10]([O:15][CH3:16])=[C:9]([O:17][CH3:18])[CH:8]=1)[NH2:28])[CH3:2]

Participants

4

Reactant 3

HCID 517165Ammonium AcetateHCID 5003444Sodium cyanoborohydrideHCID 15057242HCID 15057242, compound

Product 1

HCID 53712444HCID 53712444, compound

Procedure

In a manner similar to Preparation 21 react 2-diethylamino-1-(3,4,5-trimethoxyphenyl)ethanone with ammonium acetate and NaCNBH3 to obtain the title compound.

Workup

  1. customIn a manner similar to Preparation 21

Sources & evidence

ORD record
ord-66cb370862bc4553a3e2c0a09d5c48f1
Source dataset
uspto-grants-1990_04
Patent number
US04920116

Reaction notes

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