Hydrogen Bromide → HCID 23329122, compound

HRID 2082822Notes

Reaction equation

HRID 2082822 reaction equation
[Br:1][C:2]1[CH:14]=[CH:13][C:5]([C:6]([CH2:8][CH2:9][C:10]([OH:12])=[O:11])=[O:7])=[CH:4][C:3]=1[N+:15]([O-])=O.Br>C(O)C>[NH2:15][C:3]1[CH:4]=[C:5]([CH:13]=[CH:14][C:2]=1[Br:1])[C:6]([CH2:8][CH2:9][C:10]([OH:12])=[O:11])=[O:7]

Participants

4

Reactant 2

HCID 260Hydrogen BromideHCID 19989839HCID 19989839, compound

Product 1

HCID 23329122HCID 23329122, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

A solution of 3-(4-bromo-3-nitrobenzoyl)propionic acid in ethanol was treated with ion filings and aqueous hydrobromic acid. The residue after evaporation under reduced pressure was treated with water to give 3-(3-amino-4-bromobenzoyl)-propionic acid.

Workup

  1. customThe residue after evaporation under reduced pressure
  2. additionwas treated with water

Sources & evidence

ORD record
ord-db2acea41d9f45fe8e0cf93c30b61c91
Source dataset
uspto-grants-1978_04
Patent number
US04082843

Reaction notes

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