1,3-Propanediamine → HCID 21332412, compound

HRID 2083352Notes

Reaction equation

HRID 2083352 reaction equation
[CH2:1]1[O:13][CH:2]1[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].[CH2:14]([NH2:18])[CH2:15][CH2:16][NH2:17]>C(O)(C)C>[CH2:14]([NH:18][CH2:1][CH:2]([OH:13])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12])[CH2:15][CH2:16][NH:17][CH2:1][CH:2]([OH:13])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]

Participants

4

Reactant 2

HCID 4281,3-PropanediamineHCID 178581,2-Epoxydodecane

Product 1

HCID 21332412HCID 21332412, compound

Reagents, catalysts & solvents 1

HCID 3776IsopropanolSolvent

Procedure

In a manner similar to that of Example 1, condensation of 1-dodecene oxide (100 g.) and 1,3-propanediamine (20.1 g.) and three recrystallizations of the resulting product from isopropyl alcohol gave N,N'-(1,3-propylene)-bis[2-hydroxydodecylamine] (I: R = CH3 (CH2)9, R' = H, X = (CH2)3, Z = H) (11.9 g., 96.0°-106.0° C.).

Sources & evidence

ORD record
ord-8235bcd9440c41d68421dd6ca23a280b
Source dataset
uspto-grants-1978_04
Patent number
US04085144

Reaction notes

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