Iodoethane → HCID 22728938, compound

HRID 2085201Notes

Reaction equation

HRID 2085201 reaction equation
[H-].[Na+].[CH3:3][O:4][CH2:5][O:6][C:7]1[C:15]2[CH:14]=[C:13]([C:16]3[O:20][C:19](=[O:21])[NH:18][N:17]=3)[O:12][C:11]=2[CH:10]=[CH:9][CH:8]=1.[CH2:22](I)[CH3:23]>>[CH2:22]([O:21][C:19]1[O:20][C:16]([C:13]2[O:12][C:11]3[CH:10]=[CH:9][CH:8]=[C:7]([O:6][CH2:5][O:4][CH3:3])[C:15]=3[CH:14]=2)=[N:17][N:18]=1)[CH3:23]

Participants

4

Reactant 3

HCID 6340IodoethaneHCID 24758Sodium hydrideHCID 22729062HCID 22729062, compound

Product 1

HCID 22728938HCID 22728938, compound

Procedure

By the reactions in the same manner as in Starting Material Synthesis Example 117 using sodium hydride (0.37 g), 5-(4-(methoxymethyloxy)benzo(b)furan-2-yl)-2,3-dihydro-1,3,4-oxadiazol-2-one (2.0 g) and ethyl iodide (0.73 ml), the title compound (1.9 g) was obtained as pale-yellow crystals.

Sources & evidence

ORD record
ord-b2db69c870724b7ebb0ae244525bf384
Source dataset
uspto-grants-2004_04
Patent number
US06720320B2

Reaction notes

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