Di-tert-butyl dicarbonate → HCID 68477709, compound

HRID 2089573Notes

Reaction equation

HRID 2089573 reaction equation
[CH3:1][C:2]1[CH:3]=[C:4]2[C:8](=[C:9]([N+:11]([O-:13])=[O:12])[CH:10]=1)[NH:7][C:6]([C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1)=[CH:5]2.[O:20](C(OC(C)(C)C)=O)[C:21]([O:23][C:24]([CH3:27])([CH3:26])[CH3:25])=O>CN(C1C=CN=CC=1)C>[C:21]([N:7]1[C:8]2[C:4](=[CH:3][C:2]([CH3:1])=[CH:10][C:9]=2[N+:11]([O-:13])=[O:12])[CH:5]=[C:6]1[C:14]1[CH:15]=[CH:16][CH:17]=[CH:18][CH:19]=1)([O:23][C:24]([CH3:27])([CH3:26])[CH3:25])=[O:20]

Participants

4

Reactant 2

HCID 90495Di-tert-butyl dicarbonateHCID 68477399HCID 68477399, compound

Product 1

HCID 68477709HCID 68477709, compound

Reagents, catalysts & solvents 1

HCID 142844-(Dimethylamino)pyridineCatalyst

Procedure

5-Methyl-7-nitro-2-phenyl-1H-indole prepared in Preparation 24, (BOC)2O and DMAP were reacted according to the same procedure as Preparation 23 to give the title compound.

Workup

  1. customwere reacted
  2. customaccording to the same procedure as Preparation 23

Sources & evidence

ORD record
ord-b540a8308a694a92a8ccfecf40504f4c
Source dataset
uspto-grants-2013_05
Patent number
US08436038B2

Reaction notes

Loading…