反应详情

A mixture of the product from step (i) (8.5 g), iron powder (14 g) in acetic acid was stirred at rt for 3 h the partitioned between EtOAc/water. The organics were separated, washed with saturated NaHCO3 solution, brine, dried and evaporated under reduced pressure, yield 4.85 g.

1. custompartitioned between EtOAc/water
2. customThe organics were separated
3. washwashed with saturated NaHCO3 solution, brine
4. customdried
5. customevaporated under reduced pressure, yield 4.85 g