反应详情

3-Chloroperoxybenzoic acid (1.6 g) was added to a solution of the product from step (iii) (2.15 g) in DCM (30 mL) at 5° C. The reaction mixture was allowed to warm to rt, stirred for 18 h and partitioned between DCM/saturated sodium bisulfate solution. The organics were separated washed with saturated NaHCO3 solution, water, dried and evaporated under reduced pressure. Yield 1.77 g

1. custompartitioned between DCM/saturated sodium bisulfate solution
2. customThe organics were separated
3. washwashed with saturated NaHCO3 solution, water
4. customdried
5. customevaporated under reduced pressure