反应详情

温度

0 °C

3-Aminopropyltriethoxysilane (1.5 g, 6.78 mmol) and triethylamine (1.03 g, 10.17 mmol) were dissolved in dry THF (7 mL) at 0° C. under nitrogen atmosphere. Acryloyl chloride (0.92 g, 10.17 mmol) in dry THF (7 mL) was slowly added to the mixture at 0° C. The resulting mixture was stirred at 0° C. for 10 h. The resulting mixture was filtered through a sintered glass filter and the filtrate was concentrated to give a product as a red oil (1.31 g, 70%). This compound was used without further purification.

1. filtrationThe resulting mixture was filtered through a sintered glass
2. filtrationfilter
3. concentrationthe filtrate was concentrated