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HRID2106608

反应详情

EQUATION

反应方程式

HRID 2106608 的结构方程式

REACTANTS

反应物

3
结构：[NH4+].[OH-]
HCID14923

Ammonium hydroxide

H5NO

结构：O=C(n1ccnc1)n1ccnc1
HCID68263

1,1'-Carbonylbis(1H-imidazole)

C7H6N4O

结构：CC(Oc1ncn(-c2ccc(Br)cc2)n1)C(=O)O
HCID15016275

未命名化合物

PRODUCTS

生成物

1
结构：CC(Oc1ncn(-c2ccc(Br)cc2)n1)C(N)=O
HCID15016289

未命名化合物

收率 53.5%

PROCEDURE

实验过程

The process was carried out as was Example 45, starting with 3 g of the compound of Example 37, 2.6 g of carbonyldiimidazole and 0.7 g of ammonium hydroxide. The product was recrystallized from ethanol to obtain 1.6 g of the desired product, m.p. 179°-181°.

WORKUP

后处理

  1. customThe product was recrystallized from ethanol