HRID2107279

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID887

Methanol

CH4O

HCID4311764

Sodium borohydride (Na(BH4))

H4BNa

HCID15053541

4-Thiazolecarboxylic acid, 2-(ethylamino)-, ethyl ester

C8H12N2O2S

PRODUCTS

生成物

HCID15053558

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

The reaction described in Preparation 17 was repeated but using 10 g of ethyl 2-ethylaminothiazole-4-carboxylate, 3.8 g of sodium borohydride, 70 ml of methanol and 150 ml of tetrahydrofuran, giving the title compound as a yellow oil.

WORKUP

后处理

customThe reaction described in Preparation 17