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HRID2108053

反应详情

EQUATION

反应方程式

HRID 2108053 的结构方程式

REACTANTS

反应物

3
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：COc1ccc(C=O)cc1
HCID31244

4-Methoxybenzaldehyde

C8H8O2

结构：COc1ccc(C2CC(=O)c3cc(O)ccc3O2)cc1
HCID11818079

6-hydroxy-2-(4-methoxyphenyl)chroman-4-one

C16H14O4

PRODUCTS

生成物

1
结构：COc1ccc(C=C2C(=O)c3cc(O)ccc3OC2c2ccc(OC)cc2)cc1
HCID54236483

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

A hot solution of 27 g of 6-hydroxy-4'-methoxyflavanone and 13.6 g of anisaldehyde in 1,400 ml of ethanol is saturated with HCl and is left for 3 hours to cool; precipitation with water gives 3-p-methoxybenzylidene-6-hydroxy-4'-methoxyflavanone, m.p. 199°-201°.

WORKUP

后处理

  1. temperatureto cool
  2. customprecipitation with water