huagongshe.com
HRID2112459

反应详情

EQUATION

反应方程式

HRID 2112459 的结构方程式

REACTANTS

反应物

2
结构：CC1CNCCN1
HCID66057

2-Methylpiperazine

C5H12N2

结构：Cc1ccccc1S(=O)(=O)n1ccc2c(Br)cccc21
HCID22015334

4-Bromo-1-[(2-methylphenyl)sulfonyl]-1H-indole

C15H12BrNO2S

PRODUCTS

生成物

1
结构：Cc1ccccc1S(=O)(=O)n1ccc2c(N3CCNC(C)C3)cccc21
HCID22015381

未命名化合物

收率 38%

PROCEDURE

实验过程

The compound was prepared from 4-bromo-1-(2-methyl-benzenesulfonyl)-1H-indole and 3-methylpiperazine according to Method 1 to give 110 mg (38%) of a white solid: 1HNMR (CD3OD) δ 7.92-6.82 (m, 9H), 3.64-3.39 (m, 5H), 3.12-3.03 (m, 1H), 2.92-2.83 (m, 1H), 2.47 (s, 3H), 1.40 (d, J=7 Hz, 3H); MS (ESI) 370.0 (M+H)+; Purity (HPLC) 94%.