HRID2113543

反应详情

EQUATION

反应方程式

HRID 2113543 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A mixture of 3 g (15.8 mmol) of 2-fluoro-6-trifluoromethylbenzonitrile, 7.5 g (87 mmol) of piperazine and 24 mL of dioxane is heated at reflux for 5 hours.

WORKUP

后处理

  1. temperatureis heated
  2. temperatureat reflux for 5 hours