m-Toluidine → HCID 10341871, compound
Reaction equation
Br[CH2:2][C:3](Br)=[O:4].[CH2:6]([NH:8][CH2:9][CH3:10])[CH3:7].[NH2:11][C:12]1[CH:17]=[CH:16][CH:15]=[C:14]([CH3:18])[CH:13]=1.[C:19]([C:23]1[CH:28]=[CH:27][C:26]([S:29](Cl)(=[O:31])=[O:30])=[CH:25][CH:24]=1)([CH3:22])([CH3:21])[CH3:20]>>[C:19]([C:23]1[CH:28]=[CH:27][C:26]([S:29]([N:11]([C:12]2[CH:13]=[C:14]([CH3:18])[CH:15]=[CH:16][CH:17]=2)[CH2:2][C:3]([N:8]([CH2:9][CH3:10])[CH2:6][CH3:7])=[O:4])(=[O:31])=[O:30])=[CH:25][CH:24]=1)([CH3:22])([CH3:20])[CH3:21]Participants
5
Procedure
prepared by reaction of 2-bromoacetyl bromide with diethylamine, m-toluidine and 4-tert-butyl-benzenesulfonyl chloride
Sources & evidence
- ORD record
- ord-b000731d30cf4b9e892eb542f55e431f
- Source dataset
- uspto-grants-2008_10
- Patent number
- US07435815B2
Reaction notes
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