Dodecylamine → HCID 70445007, compound

HRID 2118710Notes

Reaction equation

HRID 2118710 reaction equation
[CH2:1]([NH2:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].[ClH:14].O[CH:16]1[O:24][C@H:23]([CH2:25][OH:26])[C@@H:21]([OH:22])[C@H:19]([OH:20])[C@H:17]1[NH2:18]>>[ClH:14].[CH2:1]([NH:13][CH:16]1[O:24][C@H:23]([CH2:25][OH:26])[C@@H:21]([OH:22])[C@H:19]([OH:20])[C@H:17]1[NH2:18])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]

Participants

3

Reactant 2

HCID 13583DodecylamineHCID 2723635(3R,4R,5S,6R)-3-amino-6-(hydroxymethyl)oxane-2,4,5-triol hydrochloride

Product 1

HCID 70445007HCID 70445007, compound

Procedure

46 g of dodecylamine are fused at 60°, and 31 g of glucosamine hydrochloride are added with stirring. After cooling to room temperature, the product precipitates out. The solid is stirred with ether three times, filtered off with suction and then dried under high vacuum.

Workup

  1. customare fused at 60°
  2. customthe product precipitates out
  3. stirringThe solid is stirred with ether three times
  4. filtrationfiltered off with suction
  5. customdried under high vacuum

Sources & evidence

ORD record
ord-29100a8c4e2e44e684a7671dd7bd4efe
Source dataset
uspto-grants-1987_07
Patent number
US04680287

Reaction notes

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