Potassium Carbonate → HCID 15072454, compound

HRID 2118808Notes

Reaction equation

HRID 2118808 reaction equation
Cl[C:2]1[CH:16]=[CH:15][C:14]([N+:17]([O-:19])=[O:18])=[CH:13][C:3]=1[C:4]([C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][C:7]=1[Cl:12])=[O:5].[CH3:20][CH:21]1[CH2:26][CH2:25][NH:24][CH2:23][CH2:22]1.C(=O)([O-])[O-].[K+].[K+]>C(O)C>[CH3:20][CH:21]1[CH2:26][CH2:25][N:24]([C:2]2[CH:16]=[CH:15][C:14]([N+:17]([O-:19])=[O:18])=[CH:13][C:3]=2[C:4]([C:6]2[CH:11]=[CH:10][CH:9]=[CH:8][C:7]=2[Cl:12])=[O:5])[CH2:23][CH2:22]1

Participants

5

Reactant 3

HCID 11430Potassium CarbonateHCID 693814-MethylpiperidineHCID 13120762HCID 13120762, compound

Product 1

HCID 15072454HCID 15072454, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

A mixture of 0.012 mole (3.6 g) of 2,2'-dichloro-5-nitrobenzophenone, of 0.018 mole (1.8 g ) of 4-methylpiperidine and of 0.012 mole (1.7 g) of potassium carbonate in 100 cm3 of anhydrous ethanol is heated for 1 hour to reflux.

Workup

  1. temperatureto reflux

Sources & evidence

ORD record
ord-756a4787647a490a8fd3339766bcf3dd
Source dataset
uspto-grants-1987_07
Patent number
US04680402

Reaction notes

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