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HRID2118818

反应详情

EQUATION

反应方程式

HRID 2118818 的结构方程式

REACTANTS

反应物

3
结构：O=C([O-])[O-].[Ca+2]
HCID10112

Calcium carbonate

CCaO3

结构：O=C(c1ccc(Cl)cc1)c1cc([N+](=O)[O-])ccc1Cl
HCID875720

未命名化合物

结构：CCC1(C)CCNCC1
HCID17750882

4-Ethyl-4-methylpiperidine

C8H17N

PRODUCTS

生成物

1
结构：CCC1(C)CCN(c2ccc([N+](=O)[O-])cc2C(=O)c2ccc(Cl)cc2)CC1
HCID20193532

未命名化合物

收率 57.4%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(=O)N(C)C
溶剂HCID31374

Dimethylacetamide

C4H9NO

PROCEDURE

实验过程

Proceeding as indicated in example 2 with 0.0734 mole (21.7 g) of 2,4'-dichloro-5-nitro-benzophenone, 0.11 mole (18 g) of 4-ethyl4-methylpiperidine and 0.22 mole (30.4 g) of calcium carbonate in 100 cm3 of N,N-dimethyl acetamide, 16.3 g (Yield: 57%) of the expected product are obtained after re-crystallization in isopropyl ether. M.P.: 105° C.