Dodecylamine → HCID 13361730, compound

HRID 2119145Notes

Reaction equation

HRID 2119145 reaction equation
O=[CH:2][C@@H:3]([C@H:5]([C@@H:7]([C@@H:9]([CH2:11][OH:12])[OH:10])[OH:8])[OH:6])[OH:4].[CH2:13]([NH2:25])[CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24]>C(O)C>[CH2:13]([NH:25][C@@H:2]1[O:10][C@H:9]([CH2:11][OH:12])[C@@H:7]([OH:8])[C@H:5]([OH:6])[C@H:3]1[OH:4])[CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24]

Participants

4

Reactant 2

HCID 13583DodecylamineHCID 107526(2R,3S,4R,5R)-2,3,4,5,6-pentahydroxyhexanal

Product 1

HCID 13361730HCID 13361730, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

18 g of glucose were stirredd in 50 ml of ethanol at 70° C., then 18.5 g of dodecylamine were added, the mixture was heated further until it was a clear solution, allowed to cool down to room temperature and, after 20 hours, the precipitated crystals were filtered off with suction. They were washed with ethanol and ether and dried in vacuo.

Workup

  1. temperaturethe mixture was heated further until it
  2. filtrationthe precipitated crystals were filtered off with suction
  3. washThey were washed with ethanol and ether
  4. customdried in vacuo

Sources & evidence

ORD record
ord-2c7d4bc5f1ed410eb6a9d0083a58ef99
Source dataset
uspto-grants-1987_07
Patent number
US04683222

Reaction notes

Loading…