Dodecylamine → HCID 70445007, compound

HRID 2119152Notes

Reaction equation

HRID 2119152 reaction equation
[CH2:1]([NH2:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].[ClH:14].O[CH:16]1[O:24][C@H:23]([CH2:25][OH:26])[C@@H:21]([OH:22])[C@H:19]([OH:20])[C@H:17]1[NH2:18]>>[ClH:14].[CH2:1]([NH:13][CH:16]1[O:24][C@H:23]([CH2:25][OH:26])[C@@H:21]([OH:22])[C@H:19]([OH:20])[C@H:17]1[NH2:18])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]

Participants

3

Reactant 2

HCID 13583DodecylamineHCID 2723635(3R,4R,5S,6R)-3-amino-6-(hydroxymethyl)oxane-2,4,5-triol hydrochloride

Product 1

HCID 70445007HCID 70445007, compound

Procedure

46 g of dodecylamine were melted at 60° and 31 g of glucosamine hydrochloride were added with stirring. After cooling down to room temperature, the product precipitated out. The solid material was stirred thoroughly three times with ether and filtered off with suction and subsequently dried under high vacuum.

Workup

  1. additionwere added
  2. customthe product precipitated out
  3. stirringThe solid material was stirred thoroughly three times with ether
  4. filtrationfiltered off with suction
  5. customsubsequently dried under high vacuum

Sources & evidence

ORD record
ord-37b39eeb0ef34d5497aa858dca724e63
Source dataset
uspto-grants-1987_07
Patent number
US04683222

Reaction notes

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