Hydrochloric Acid → HCID 56828137, compound

HRID 2121525Notes

Reaction equation

HRID 2121525 reaction equation
[N:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][C:2]=1[C:11]([OH:13])=[O:12].OCC1(OC[C@@H](O)[C@@H](O)[C@H]1O)O.[ClH:26]>C(O)(=O)C.O=[Pt]=O>[ClH:26].[NH:1]1[CH:10]2[CH:5]([CH2:6][CH2:7][CH2:8][CH2:9]2)[CH2:4][CH2:3][CH:2]1[C:11]([OH:13])=[O:12]

Participants

6

Reactant 3

HCID 313Hydrochloric AcidHCID 7124Quinaldic AcidHCID 441036D-Psicose

Product 1

HCID 56828137HCID 56828137, compound

Reagents, catalysts & solvents 2

HCID 345198Adams' catalystCatalystHCID 176Acetic AcidSolvent

Procedure

A mixture of PtO2 (25 wt. %) and 2-quinolinecarboxylic acid (Aldrich) in acetic acid was hydrogenated at RT under 60 Psi overnight. The reaction mixture was stripped to dryness. Concentrated HCl was added and stripped to dryness to give the title compound as a white solid.

Sources & evidence

ORD record
ord-e474eab8635e4beb8eb76c63c16f701b
Source dataset
uspto-grants-2004_02
Patent number
US06696438B2

Reaction notes

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