huagongshe.com
HRID215865

反应详情

EQUATION

反应方程式

HRID 215865 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)OC(=O)N[C@@H]1CCNC1
HCID1514397

tert-Butyl (3R)-pyrrolidin-3-ylcarbamate

C9H18N2O2

结构：CC(C)(C)OC(=O)NC1CCC(NC(=O)Oc2ccccc2)CC1
HCID67022954

(4-tert-Butoxycarbonylamino-cyclohexyl)-carbamic acid phenyl ester

C18H26N2O4

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)NC1CCC(NC(=O)N2CC[C@@H](NC(=O)OC(C)(C)C)C2)CC1
HCID67023870

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN1CCCC1=O
溶剂HCID13387

N-Methyl-2-pyrrolidone

C5H9NO

CONDITIONS

反应条件

温度
100 °C

PROCEDURE

实验过程

(4-tert-Butoxycarbonylamino-cyclohexyl)-carbamic acid phenyl ester (1 eq.) and (R)-pyrrolidin-3-yl-carbamic acid tert-butyl ester (1 eq.) are dissolved in NMP and heated at 100° C. for 1 hour.