Adipoyl chloride → HCID 22754107, compound

HRID 2163152Notes

Reaction equation

HRID 2163152 reaction equation
[NH2:1][C:2]1[C:3]([I:20])=[C:4]([C:13]([NH:15][CH2:16][CH:17]([OH:19])[CH3:18])=[O:14])[C:5]([I:12])=[C:6]([C:10]=1[I:11])[C:7]([OH:9])=[O:8].[C:21](Cl)(=[O:29])[CH2:22][CH2:23][CH2:24][CH2:25][C:26](Cl)=[O:27]>CC(N(C)C)=O>[C:21]([NH:1][C:2]1[C:3]([I:20])=[C:4]([C:13]([NH:15][CH2:16][CH:17]([OH:19])[CH3:18])=[O:14])[C:5]([I:12])=[C:6]([C:10]=1[I:11])[C:7]([OH:9])=[O:8])(=[O:29])[CH2:22][CH2:23][CH2:24][CH2:25][C:26]([NH:1][C:2]1[C:3]([I:20])=[C:4]([C:13]([NH:15][CH2:16][CH:17]([OH:19])[CH3:18])=[O:14])[C:5]([I:12])=[C:6]([C:10]=1[I:11])[C:7]([OH:9])=[O:8])=[O:27]

Participants

4

Reactant 2

HCID 61034Adipoyl chlorideHCID 22754106HCID 22754106, compound

Product 1

HCID 22754107HCID 22754107, compound

Reagents, catalysts & solvents 1

HCID 31374DimethylacetamideSolvent

Procedure

Analogously to Example 10, 5-amino-N-(2-hydroxypropyl)2,4,6-triiodoisophthalamic acid is reacted with hexanedioic acid dichloride in dimethylacetamide and then worked up. The thus-obtained product melts at 284°-285° C., with decomposition.

Sources & evidence

ORD record
ord-3fa2590410754481bd1d9a14adbdb5cf
Source dataset
uspto-grants-1979_01
Patent number
US04132731

Reaction notes

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