反应详情

A mixture of 45 g (0.5 mole) carbohydrazide, 85 g NaHCO3 (1.0 mole) and 250 ml methanol was stirred and 128.5 g (1.0 mole) ethane sulfonyl chloride was dropped in. The temperature rose from 25° C to 45° C during the reaction which took 1 hour. Stirring was continued for two hours. The produce was filtered, washed and dried. Yield: 145.9 g m.p. 195° C.

1. customThe temperature rose from 25° C to 45° C during the reaction which
2. stirringStirring
3. waitwas continued for two hours
4. filtrationThe produce was filtered
5. washwashed
6. customdried