HRID2167873

反应详情

EQUATION

反应方程式

HRID 2167873 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A mixture of 4-benzyl-2-{4-[2-(2,6-dichloro-phenyl)-vinyl]-phenyl}-morpholine (0.54 g; 1.27 mmol) and palladium hydroxide (0.04 g; 0.25 mmol) in MeOH (25 mL) was treated with H2, at normal pressure, overnight. The resulting mixture was filtered over Kieselguhr and the solvents evaporated to afford 2-(4-phenethyl-phenyl)-morpholine (0.34 g).

WORKUP

后处理

  1. additionwas treated with H2, at normal pressure, overnight
  2. filtrationThe resulting mixture was filtered over Kieselguhr
  3. customthe solvents evaporated