Citric Acid → 5-(2-(4-Hydroxyphenyl)Ethenyl)Benzene-1,3-Diol

HRID 2170241Notes

Reaction equation

HRID 2170241 reaction equation
N[CH2:2][CH2:3]S(O)(=O)=O.[CH3:8][C:9]1[N+](CC2C(N)=NC(C)=NC=2)=CS[C:10]=1[CH2:23][CH2:24][OH:25].[N+]([O-])([O-])=[O:27].C([O-])(=O)[C:31]1[CH:36]=[CH:35][CH:34]=CC=1.[Na+].C(O)(=O)[CH2:41][C:42](CC(O)=O)([C:44](O)=O)[OH:43].Cl>C(O)C.O>[C:10]1([CH:9]=[CH:8][C:3]2[CH:2]=[CH:34][C:35]([OH:27])=[CH:36][CH:31]=2)[CH:23]=[C:24]([OH:25])[CH:44]=[C:42]([OH:43])[CH:41]=1

Participants

8

Reactant 5

HCID 311Citric AcidHCID 313Hydrochloric AcidHCID 1123TaurineHCID 10762Thiamine NitrateHCID 517055Sodium Benzoate

Product 1

HCID 50565-(2-(4-Hydroxyphenyl)Ethenyl)Benzene-1,3-Diol

Reagents, catalysts & solvents 2

HCID 702EthanolSolventHCID 962WaterSolvent

Procedure

1 g of the UHA4002 and 0.2 g of the UHA4003 obtained by the method of Example 8 were dissolved in 10 mL of ethanol, 20 g of taurine, 0.12 g of vitamin B1 nitrate, 0.6 g of sodium benzoate, 4 g of citric acid, 60 g of sugar, and 10 g of polyvinyl pyrrolidone were all dissolved in purified water, and then the solution was diluted in a measuring cylinder to 1000 ml. The pH was adjusted to 3.2 using dilute hydrochloric acid. 50 ml of 1000 ml of the obtained solution was charged into a glass bottle, and then sterilized at 80° C. for 30 minutes, thereby completing a drink agent which is a quasi drug. The drink agent can be effectively utilized as a quasi drug aiming at reducing the risk of infectious diseases in addition to the purpose of supply of nutrients.

Workup

  1. custom1 g of the UHA4002 and 0.2 g of the UHA4003 obtained by the method of Example 8
  2. additionthe solution was diluted in a measuring cylinder to 1000 ml
  3. additionin addition to the purpose of supply of nutrients

Sources & evidence

ORD record
ord-e25a8ff63f4648d8be18bf71300006b7
Source dataset
uspto-grants-2015_06
Patent number
US09051245B2

Reaction notes

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