huagongshe.com
HRID2172347

反应详情

EQUATION

反应方程式

HRID 2172347 的结构方程式

REACTANTS

反应物

3
结构：C=O
HCID712

Formaldehyde

CH2O

结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：CCOC(=O)Cc1ccc(Br)cc1
HCID7020609

Ethyl 4-bromophenylacetate

C10H11BrO2

PRODUCTS

生成物

1
结构：C=C(C(=O)OCC)c1ccc(Br)cc1
HCID11470828

Ethyl 2-(4-bromophenyl)acrylate

C11H11BrO2

AUXILIARIES

试剂、催化剂与溶剂

2
结构：CCCC[N+](CCCC)(CCCC)CCCC.[I-]
催化剂HCID67553

Tetrabutylammonium Iodide

C16H36IN

结构：Cc1ccccc1
溶剂HCID1140

Toluene

C7H8

PROCEDURE

实验过程

is prepared by treating a toluene solution of (4-bromo-phenyl)-acetic acid ethyl ester with paraformaldehyde, potassium carbonate, tetrabutylammonium iodide according to the following literature: H. Stalder, M. Boes Chimia 2000, 54, 669-671.

WORKUP

后处理

  1. customis prepared