Hydrochloric Acid → HCID 22476022, compound

HRID 2184239Notes

Reaction equation

HRID 2184239 reaction equation
C1(=O)N[C:4](=[O:6])[C:3]2=[CH:7][CH:8]=[CH:9][CH:10]=[C:2]12.NN.Cl.N[CH2:16][C:17]1[CH:18]=[N:19]C(C#N)=N[CH:22]=1.Cl>>[NH2:19][CH2:18][C:17]1[CH:16]=[CH:22][C:17]([C:18]#[N:19])=[CH:16][C:22]=1[O:6][CH2:4][C:3]1[CH:2]=[CH:10][CH:9]=[CH:8][CH:7]=1

Participants

5

Reactant 4

HCID 313Hydrochloric AcidHCID 6809PhthalimideHCID 9321HydrazineHCID 22476050182287-56-5

Product 1

HCID 22476022HCID 22476022, compound

Procedure

Synthesis took place via the stage of the corresponding phthalimide as in Example 3.(f). The hydrazine cleavage was carried out as in Example 3.(g). The free amine was generated at pH 9-10 from the initially produced hydrochloride and was extracted from the aqueous solution with ether.

Workup

  1. customSynthesis
  2. extractionwas extracted from the aqueous solution with ether

Sources & evidence

ORD record
ord-16c549c9fd214fc1aad58465f0faefe6
Source dataset
uspto-grants-2005_05
Patent number
US06900319B2

Reaction notes

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