HRID2185131

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID13139

Diethyl phosphorochloridate

C4H10ClO3P

HCID178418439

未命名化合物

PRODUCTS

生成物

HCID4254391

2-diethylphosphonothiophene

C8H13O3PS

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

A solution of 1.0 mmol 2-thienyl lithium in THF was treated with 1.0 mmol diethyl chlorophosphate at −78° C. for 1 h. Extraction and chromatography gave diethyl 2-thiophenephosphonate as a clear oil.

WORKUP

后处理

extractionExtraction and chromatography