反应详情

To a solution of 3-(isopropoxy)-5,6,7,8-tetrahydro-1-naphthalenecarboxylic acid (0.318 g, 1.36 mmol) in DCM (5 mL) was added oxalyl chloride (0.15 mL, 1.70 mmol) and 2 drops of DMF. The mixture was stirred at room temperature for 3 h. The solvent was removed in vacuo and the 3-(isopropoxy)-5,6,7,8-tetrahydro-1-naphthalenecarbonyl chloride was used without purification.

1. customThe solvent was removed in vacuo
2. customthe 3-(isopropoxy)-5,6,7,8-tetrahydro-1-naphthalenecarbonyl chloride was used without purification