HRID2191802

反应详情

EQUATION

反应方程式

HRID 2191802 的结构方程式

PROCEDURE

实验过程

Trifluoroacetic acid 7.5 mL solution of tert-butyl 2-(4-fluoroanilino)-4-(2-(2-methoxyphenyl)ethyl)benzoate 0.11 g was stirred at room temperature for 2 hours. The solvent was removed under reduced pressure,diisopropyl ether was added to the obtained residue, and solid matter was filtrated to give 2-(4-fluoroanilino)-4-(2-(2-methoxyphenyl)ethyl)benzoic acid 12 mg of a white solid.

WORKUP

后处理

  1. customThe solvent was removed under reduced pressure,diisopropyl ether
  2. additionwas added to the obtained residue, and solid matter
  3. filtrationwas filtrated