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HRID2196998

反应详情

EQUATION

反应方程式

HRID 2196998 的结构方程式

REACTANTS

反应物

4
结构：[H-].[Na+]
HCID24758

Sodium hydride

HNa

结构：C1COCCOCCOCCOCCO1
HCID36336

1,4,7,10,13-Pentaoxacyclopentadecane

C10H20O5

结构：O=S(=O)(Cl)c1cccnc1
HCID3164136

Pyridine-3-sulfonyl chloride

C5H4ClNO2S

结构：CS(=O)(=O)c1ccccc1-c1cc(C=O)c[nH]1
HCID86630991

未命名化合物

PRODUCTS

生成物

1
结构：CS(=O)(=O)c1ccccc1-c1cc(C=O)cn1S(=O)(=O)c1cccnc1
HCID86630996

未命名化合物

PROCEDURE

实验过程

By a similar operation as in Reference Example 154 and using sodium hydride (60% in oil, 40 mg), 5-[2-(methylsulfonyl)phenyl]-1H-pyrrole-3-carbaldehyde (88.9 mg), 15-crown-5 (94.4 mg) and pyridin-3-ylsulfonyl chloride (69.7 mg), the title compound was obtained as a colorless amorphous form (yield 72.0 mg, 52%).