反应详情

温度

10 °C

The product from Example 4a (1.00 g, 3.51 mmol) and 3-Amino-benzenethiol (658 mg, 5.26 mmol) were dissolved in DMF to which was added K2CO3 (848 mg, 6.14 mmol). The reaction mixture was then heated to 10° C. for 16 hrs. Reaction mixture was then cooled to room temperature, diluted with water and extracted with ethyl acetate providing the title compound (650 mg, 71%).

1. customReaction mixture
2. temperaturewas then cooled to room temperature
3. extractionextracted with ethyl acetate providing the title compound (650 mg, 71%)