HRID2198299

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID712

Formaldehyde

CH2O

HCID6422

未命名化合物

HCID75331

m-Chlorophenylhydrazine hydrochloride

C6H8Cl2N2

HCID13994547

4,4-Diethoxy-N-methylbutan-1-amine

C9H21NO2

HCID21071655

未命名化合物

PRODUCTS

生成物

结构：Cc1ccc(C(O)Cn2c3c(c4ccc(Cl)cc42)CCN(C)C3)cn1

HCID44242180

2-(7-chloro-2-methyl-3,4-dihydro-1H-pyrido[3,4-b]indol-9(2H)-yl)-1-(6-methylpyridin-3-yl)ethanol

C20H22ClN3O

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID6342

Acetonitrile

C2H3N

溶剂HCID24758

Sodium hydride

HNa

溶剂HCID15713588

未命名化合物

溶剂HCID57930478

未命名化合物

PROCEDURE

实验过程

The title compound is prepared by following General Methods 3, 4 and 8 by using 3-chlorophenylhydrazine hydrochloride and 4,4-diethoxy-N-methylbutan-1-amine (General Method 3), 2-(6-chloro-1H-indol-3-yl)-N-methylethanamine, formaldehyde and TFA in acetonitrile (General Method 4) and 7-chloro-2,3,4,9-tetrahydro-2-methyl-1H-pyrido[3,4-b]indole, 2-methyl-5-(oxiran-2-yl)pyridine and NaH (General Method 8).