HRID2202825

反应详情

EQUATION

反应方程式

HRID 2202825 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Compound 107-1 (429 mg, 1.42 mmol) was dissolved in THF (10 mL) and treated with potassium trimethylsilanolate (273 mg, 2.13 mmol). After stirring for 1 h, the mixture was concentrated in vacuo to provide 107-2 that was used directly in the next step.

WORKUP

后处理

  1. concentrationthe mixture was concentrated in vacuo
  2. customto provide 107-2 that