HRID22090

反应详情

EQUATION

反应方程式

HRID 22090 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

CONDITIONS

反应条件

温度
90 °C

PROCEDURE

实验过程

1.74 g of p-hydroxy cinnamic acid and 4.0 g of glycidol were dissolved in 2 ml of DMSO, and catalytic amount of hydrochloric acid was added. The solution was heated to 90° C., heating and agitation were carried out for 1 hour, neutralized by adding sodium hydroxide and then the adduct of cinnamic acid and glycerin was obtained.

WORKUP

后处理

  1. temperatureheating