3-Bromopropylamine hydrobromide → tert-butyl N-(3-bromopropyl)carbamate

HRID 2213519Notes

Reaction equation

HRID 2213519 reaction equation
Br.[Br:2][CH2:3][CH2:4][CH2:5][NH2:6].[O:7](C(OC(C)(C)C)=O)[C:8]([O:10][C:11]([CH3:14])([CH3:13])[CH3:12])=O>ClCCl>[Br:2][CH2:3][CH2:4][CH2:5][NH:6][C:8](=[O:7])[O:10][C:11]([CH3:14])([CH3:13])[CH3:12]

Participants

4

Reactant 2

HCID 787013-Bromopropylamine hydrobromideHCID 90495Di-tert-butyl dicarbonate

Product 1

HCID 4460490tert-butyl N-(3-bromopropyl)carbamate

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

was prepared from 3-bromopropylamine hydrobromide and BOC2O in the presence of base in dichloromethane.

Sources & evidence

ORD record
ord-cd3c0456f99f4bdfa773966ab7a1c015
Source dataset
uspto-grants-2006_09
Patent number
US07105544B2

Reaction notes

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