4-Isopropylaniline → HCID 21957913, compound

HRID 2213601Notes

Reaction equation

HRID 2213601 reaction equation
[Br:1][C:2]1[CH:9]=[CH:8][C:5]([CH:6]=O)=[CH:4][CH:3]=1.[CH:10]([C:13]1[CH:19]=[CH:18][C:16]([NH2:17])=[CH:15][CH:14]=1)([CH3:12])[CH3:11]>>[Br:1][C:2]1[CH:9]=[CH:8][C:5]([CH2:6][NH:17][C:16]2[CH:18]=[CH:19][C:13]([CH:10]([CH3:12])[CH3:11])=[CH:14][CH:15]=2)=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 74644-IsopropylanilineHCID 707414-Bromobenzaldehyde

Product 1

HCID 21957913HCID 21957913, compoundYield 57.6%

Procedure

By the reaction and treatment in the same manner as in Preparation Example 1 using 4-bromobenzaldehyde (1.9 g) and 4-isopropylaniline (1.4 g) as starting materials, [(4-bromophenyl)methyl](4-isopropylphenyl)amine (1.8 g) was obtained. melting point: 30° C.

Workup

  1. customBy the reaction and treatment in the same manner

Sources & evidence

ORD record
ord-457a0d25ce2e444c937622570dd53cf4
Source dataset
uspto-grants-2006_09
Patent number
US07105567B2

Reaction notes

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