HRID2216351

反应详情

EQUATION

反应方程式

HRID 2216351 的结构方程式

PROCEDURE

实验过程

A mixture of 505 mg of 2-benzyl-1-methoxymethyloxy-4-(2-pyrrolidinon-1-yl)benzene and 5 ml of trifluoroacetic acid was stirred at room temperature for 1 hour. The reaction mixture was evaporated, and the residue was purified by silica gel column chromatography with 30–60% ethyl acetate/hexane, to give 320 mg of the title compound.

WORKUP

后处理

  1. customThe reaction mixture was evaporated
  2. customthe residue was purified by silica gel column chromatography with 30–60% ethyl acetate/hexane