HRID2216351
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
A mixture of 505 mg of 2-benzyl-1-methoxymethyloxy-4-(2-pyrrolidinon-1-yl)benzene and 5 ml of trifluoroacetic acid was stirred at room temperature for 1 hour. The reaction mixture was evaporated, and the residue was purified by silica gel column chromatography with 30–60% ethyl acetate/hexane, to give 320 mg of the title compound.
WORKUP
后处理
- customThe reaction mixture was evaporated
- customthe residue was purified by silica gel column chromatography with 30–60% ethyl acetate/hexane