反应详情

Lithium hydroxide monohydrate (0.089 g) was added to a mixture of 4-ethoxycarbonyl-2,6-dimethylphenylboronic acid (0.047 g), water (1 mL) and 1,4-dioxane (1 mL), and the mixture was stirred at room temperature overnight. To the reaction mixture was added 2 mol/L hydrochloric acid (1.5 mL), and the solvent was evaporated under reduced pressure. The residue was washed with water to afford the title compound (0.023 g).

1. customthe solvent was evaporated under reduced pressure
2. washThe residue was washed with water