HRID2221081

反应详情

EQUATION

反应方程式

HRID 2221081 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

2-Oxo-[1,4′]bipiperidinyl-1′-carboxylic acid benzyl ester (2.5 g) and Pearlman's catalyst (0.50 g) was stirred in ethanol (30 mL) under hydrogen (1 atm). After 20 hours the reaction as filtered through celite and concentrated. The title compound was obtained as a white solid (1.45 g). MS: m/z=183 (M+H).

WORKUP

后处理

  1. customAfter 20 hours the reaction
  2. filtrationas filtered through celite and
  3. concentrationconcentrated