HRID2223207

反应详情

EQUATION

反应方程式

HRID 2223207 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A mixture of 0.67 g (2.0 mmol) of methyl 6-benzyloxy-5-nitro-indole-2-carboxylate, 60 ml of tetrahydrofuran and 0.1 g of 10% Pd/C catalyst is hydrogenated for 5 h. The catalyst is filtered off and the filtrate containing the title compound is used immediately in the next step.

WORKUP

后处理

  1. filtrationThe catalyst is filtered off
  2. additionthe filtrate containing the title compound