HRID2226829

反应详情

EQUATION

反应方程式

HRID 2226829 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a mixture of ethyl acetate (50 ml) and aqueous potassium carbonate (20 ml), 3-(3-trifluoromethyl-4-fluorophenyl)-5-methyl-2-iminothiazoline hydrochloride (1 g) was added; and the mixture was stirred. The organic layer was isolated and dried over anhydrous magnesium sulfate. The solvent was removed under reduced pressure to give 0.7 g of 3-(3-trifluoromethyl-4-fluorophenyl)-5-methyl-2-iminothiazoline as an oil.

WORKUP

后处理

  1. additionwas added
  2. customThe organic layer was isolated
  3. dry with materialdried over anhydrous magnesium sulfate
  4. customThe solvent was removed under reduced pressure