Homoveratrylamine → HCID 13364782, compound

HRID 2231864Notes

Reaction equation

HRID 2231864 reaction equation
[C:1]1(=[O:19])[N:5]([CH2:6][C:7](=O)[CH2:8][CH2:9][C:10](=O)[CH3:11])[C:4](=[O:14])[C:3]2=[CH:15][CH:16]=[CH:17][CH:18]=[C:2]12.[CH3:20][O:21][C:22]1[CH:23]=[C:24]([CH2:30][CH2:31][NH2:32])[CH:25]=[CH:26][C:27]=1[O:28][CH3:29]>C(O)(=O)C>[CH3:20][O:21][C:22]1[CH:23]=[C:24]([CH2:30][CH2:31][N:32]2[C:10]([CH3:11])=[CH:9][CH:8]=[C:7]2[CH2:6][N:5]2[C:4](=[O:14])[C:3]3=[CH:15][CH:16]=[CH:17][CH:18]=[C:2]3[C:1]2=[O:19])[CH:25]=[CH:26][C:27]=1[O:28][CH3:29]

Participants

4

Reactant 2

HCID 8421HomoveratrylamineHCID 123484512-(2,5-Dioxohexyl)-1H-isoindole-1,3(2H)-dione

Product 1

HCID 13364782HCID 13364782, compound

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

13.0 g (0.05 mol) of 6-phthalimido-2,5-hexanedione and 9.1 g (0.05 mol) of 2-(3,4-dimethoxyphenyl)-ethylamine are stirred in 250 ml of acetic acid at 80° C. for 7 hours. After working up as in Example 1, 7.3 g of product are obtained.

Workup

  1. customare obtained

Sources & evidence

ORD record
ord-2fbd7fc62f32474fb5b53eece0e736f2
Source dataset
uspto-grants-1988_11
Patent number
US04785010

Reaction notes

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