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HRID2240929

反应详情

EQUATION

反应方程式

HRID 2240929 的结构方程式

REACTANTS

反应物

3
结构：CCOCC
HCID3283

Diethyl Ether

C4H10O

结构：CCCC[N+](CCCC)(CCCC)CCCC.[F-]
HCID2724141

Tetra-n-butylammonium fluoride

C16H36FN

结构：CC(C)[Si](C#Cc1ccc(F)c(O)c1)(C(C)C)C(C)C
HCID59305361

未命名化合物

PRODUCTS

生成物

1
结构：C#Cc1ccc(F)c(O)c1
HCID59305335

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1CCOC1
溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

2-fluoro-5-((triisopropylsilyl)ethynyl)phenol is dissolved in THF and tetrabutyl ammoniumflouride is added. The solution is stirred overnight at RT. Et2O is added and the solution is washed with H2O, Brine, dried, and the solvent removed. This material is used without any further purification.

WORKUP

后处理

  1. washthe solution is washed with H2O, Brine
  2. customdried
  3. customthe solvent removed
  4. customThis material is used without any further purification