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HRID2241994

反应详情

EQUATION

反应方程式

HRID 2241994 的结构方程式

REACTANTS

反应物

3
结构：CC(=O)O[BH-](OC(C)=O)OC(C)=O.[Na+]
HCID5049666

Sodium triacetoxyborohydride

C6H10BNaO6

结构：Clc1ccc(N2CCNCC2)c2ncccc12
HCID58975503

未命名化合物

结构：O=C1CCN(c2cccc3cccnc23)CC1
HCID59204842

未命名化合物

PRODUCTS

生成物

1
结构：Clc1ccc(N2CCN(C3CCN(c4cccc5cccnc45)CC3)CC2)c2ncccc12
HCID12004167

未命名化合物

PROCEDURE

实验过程

Using the synthetic methods described in previous examples, 5-chloro-8-(piperazin-1-yl)quinoline (Step 3) and 1-quinolin-8-yl-piperidin-4-one (Example A, Step 5, above) were reacted with sodium triacetoxyborohydride to give the desired product as a beige solid; MP. 201-203° C.; MS (ES) m/z (relative intensity) 459 (M+H)+ (100).