Methanesulfonic Acid → HCID 178427486, compound

HRID 2242155Notes

Reaction equation

HRID 2242155 reaction equation
C[C:2]1[CH:6]=[C:5](C)[N:4]([C:8](=N)[NH:9][S:10]([C:13]2[CH:18]=[CH:17][C:16]([CH3:19])=[CH:15][CH:14]=2)(=[O:12])=[O:11])[N:3]=1.CS(O)(=O)=O.C(N)CC>>[NH2:3][CH2:2][CH2:6][CH2:5][NH:4][CH:8]=[N:9][S:10]([C:13]1[CH:14]=[CH:15][C:16]([CH3:19])=[CH:17][CH:18]=1)(=[O:12])=[O:11]

Participants

4

Reactant 3

HCID 6395Methanesulfonic AcidHCID 7852PropylamineHCID 178427489N-[(3,5-dimethylpyrazol-1-yl)-iminomethyl]-4-methylbenzene-sulfonamide

Product 1

HCID 178427486HCID 178427486, compound

Procedure

The compound of Example 10 was prepared according to the accompanying synthesis procedure from 0.5 ml of N-[(3,5-dimethylpyrazol-1-yl)-iminomethyl]-4-methylbenzene-sulfonamide solution (0.2 M, acetonitrile) with 19 mg of methanesulfonic acid and 0.5 ml of n-propylamine solution (1.0 M, acetonitrile) and filed in a substance databank. Calculated mol. wt. 255.34; found mol. wt. (M+H) 256.2; 511.0 (Dimer)

Sources & evidence

ORD record
ord-341e68069d0b41dab3b3aec53b53a247
Source dataset
uspto-grants-2010_03
Patent number
US07671074B2

Reaction notes

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